2-Methylphloroglucinol → HCID 19085796, compound

HRID 962638Notes

Reaction equation

HRID 962638 reaction equation
[OH:1][C:2]1[CH:3]=C(O)C=[C:6]([OH:9])[C:7]=1[CH3:8].[ClH:11].[CH2:12]([N:19]1[CH2:24][CH2:23][C:22](=O)[CH:21]([C:26]([O:28][CH2:29][CH3:30])=[O:27])[CH2:20]1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[ClH:11].[CH2:12]([N:19]1[CH2:24][CH2:23][C:22]2[C:3]3[C:2]([OH:1])=[C:7]([CH3:8])[C:6]([OH:9])=[CH:30][C:29]=3[O:28][C:26](=[O:27])[C:21]=2[CH2:20]1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 666062-MethylphloroglucinolHCID 102623Ethyl 1-benzyl-4-oxopiperidine-3-carboxylate hydrochloride

Product 1

HCID 19085796HCID 19085796, compoundYield 24%

Procedure

Prepared by the procedure of Example 1 from 3,5-dihydroxy-4-methylphenol and ethyl 1-benzyl-4-oxo-3-piperidinecarboxylate hydrochloride. The crude product was converted to the hydrochloride salt. Yield 24%; mp 293°-299° C.

Sources & evidence

ORD record
ord-837a8ca52b67427e818bec32828725a5
Source dataset
uspto-grants-1998_06
Patent number
US05760050

Reaction notes

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