HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethoxyphenol → 3-Benzyl-7,8-dimethoxy-1,2,3,4-tetrahydro-chromeno[3,4-c]pyridin-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethoxyphenol | HCID 78828 | — |
| Reactant | Methyl 1-benzyl-4-oxopiperidine-3-carboxylate hydrochloride | HCID 107479 | — |
| Product | 3-Benzyl-7,8-dimethoxy-1,2,3,4-tetrahydro-chromeno[3,4-c]pyridin-5-one | HCID 10665626 | 35% |
Reaction Steps
Prepared by the procedure of Example 1 from 2,3-dimethoxyphenol and methyl 1-benzyl-4-oxo-3-piperidine-carboxylate hydrochloride. Yield 35%; mp 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05760050 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-652eba3afc2a47e7bbf74cccd53820e9 |
| Source note | uspto-grants-1998_06 |