Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cumylamine → N-(1-Methyl-1-phenylethyl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cumylamine | HCID 68509 | — |
| 반응물 | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| 생성물 | N-(1-Methyl-1-phenylethyl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 15380257 | 75% |
반응 단계
A procedure similar to that described in Example 3(b) was repeated, except that S-2-pyridyl 3-cyanoandrosta-3,5-diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 1-methyl-1-phenylethylamine were used as starting materials, in relative proportions similar to those used in that Example, to give the title compound in a yield of 75%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05760025 |
| 출처 데이터셋 | uspto-grants-1998_06 |
| ORD ID | ord-12bd1127f99a46919113c5e36c3f95d8 |
| 출처 메모 | uspto-grants-1998_06 |