HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4'-Dimethoxybenzhydrylamine → N-(4,4'-Dimethoxybenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4'-Dimethoxybenzhydrylamine | HCID 350042 | — |
| Reactant | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| Product | N-(4,4'-Dimethoxybenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamid | HCID 15380274 | 79% |
Reaction Steps
Following a procedure similar to that described in Example 3(b), but using S-2-pyridyl 3-cyanoandrosta-3,5-diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 4,4'-dimethoxybenzhydrylamine (prepared as described in Preparation 14) as starling materials, in relative proportions similar to those used in that Example, the title compound was obtained in a yield of 79%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05760025 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-29f0a16f0ca74c7ebd25ac26da0ea535 |
| Source note | uspto-grants-1998_06 |