HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Methoxyphenyl)-1-phenylmethanamine → N-(4-Methoxybenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Methoxyphenyl)-1-phenylmethanamine | HCID 350041 | — |
| Reactant | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| Product | N-(4-Methoxybenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 15380278 | 82% |
Reaction Steps
Following a procedure similar to that described in Example 3(b), but using S-2-pyridyl 3-cyanoandrosta-3,5-diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 4-methoxybenzhydrylamine (prepared as described in Preparation 15) as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained in a yield of 82%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05760025 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-8f2413f6196840a593b681a0997f7854 |
| Source note | uspto-grants-1998_06 |