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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 962914Generated: October 30, 2026

Chlorine → HCID 19604208, compound

https://huagongshe.com/reaction/962914

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorineHCID 24526—
ReactantHCID 19604218HCID 19604218—
SolventMethanolHCID 887—
ProductHCID 19604208HCID 19604208—

Reaction Steps

This compound was also obtained in 28 percent yield by chlorinating 5-succinoyl-2-pyridone methyl ester (obtained analogously to Example 7 from 5-succinoyl-2-pyridone and methanol/sulfuric acid) using chlorine in methanol. The main product obtained (70 percent yield) was methyl 4-(3,5-dichloro-2-methoxy-6-oxo-1,2,3,6-tetrahydropyridin-3-yl)-4-oxobutyrate, which was characterized by the following data:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05760236
Source datasetuspto-grants-1998_06
ORD IDord-30b42a97760044b68c1518f973eafd3e
Source noteuspto-grants-1998_06