HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 19604208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 19604218 | HCID 19604218 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19604208 | HCID 19604208 | — |
Reaction Steps
This compound was also obtained in 28 percent yield by chlorinating 5-succinoyl-2-pyridone methyl ester (obtained analogously to Example 7 from 5-succinoyl-2-pyridone and methanol/sulfuric acid) using chlorine in methanol. The main product obtained (70 percent yield) was methyl 4-(3,5-dichloro-2-methoxy-6-oxo-1,2,3,6-tetrahydropyridin-3-yl)-4-oxobutyrate, which was characterized by the following data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05760236 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-30b42a97760044b68c1518f973eafd3e |
| Source note | uspto-grants-1998_06 |