HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl glycidyl ether → HCID 21845233, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl glycidyl ether | HCID 31217 | — |
| Reactant | 4-(4-Hydroxyphenyl)thiomorpholine 1,1-Dioxide | HCID 21845223 | — |
| Catalyst | Phosphonium, ethyltriphenyl-, bromide (1:1) | HCID 73727 | — |
| Product | HCID 21845233 | HCID 21845233 | 58.3% |
Reaction Steps
4-(1,1-dioxo-thiomorpholin-4-yl)phenol (2.3 g, 10 mmol), phenylglycidyl ether (1.5 g, 10 mmol) and ethyltriphenylphosphonium bromide (0.1 g) are reacted and purified as described for compound 102 to afford a light yellow liquid 2.2 g (58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763144 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-3a85db966f3541b8b801dcdc9fe4b779 |
| Source note | uspto-grants-1998_06 |