HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethoxybenzyl chloride → 1-[4-Acetylamino-5-bromo-2-(3,5-dimethoxybenzyloxy)phenyl]-5-bromopentan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethoxybenzyl chloride | HCID 2758395 | — |
| Reactant | 1-(4-Acetylamino-5-chloro-2-hydroxyphenyl)-5-chloropentan-1-one | HCID 19081879 | — |
| Reactant | 1-(4-Acetylamino-5-bromo-2-hydroxyphenyl)-5-bromopentan-1-one | HCID 19081952 | — |
| Product | 1-[4-Acetylamino-5-bromo-2-(3,5-dimethoxybenzyloxy)phenyl]-5-bromopentan-1-one | HCID 19081955 | — |
Reaction Steps
Proceeding as in Example 4, Step (b), but replacing iodomethane with 3,5-dimethoxybenzylchloride and 1-(4-acetylamino-5-chloro-2-hydroxyphenyl)-5-chloropentan-1-one with 1-(4-acetylamino-5-bromo-2-hydroxyphenyl)-5-bromo-pentan-1-one, gave 1-[4-acetylamino-5-bromo-2-(3,5-dimethoxybenzyloxy)phenyl]-5-bromopentan-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763458 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-5554108108704e048f88d79e8c2a69f2 |
| Source note | uspto-grants-1998_06 |