HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylstannane → HCID 19082567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylstannane | HCID 5948 | — |
| Reactant | HCID 19082572 | HCID 19082572 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19082567 | HCID 19082567 | 90.1% |
Reaction Steps
Ethyl 2,2,6,6,7,7,8,8,9,9,9-undecafluorononanoate (17.3 g, 90% yield) was prepared from ethyl 4-iodo-2,2,6,6,7,7,8,8,9,9,9-undecafluorononanoate (25.5 g, 50 mmol), tributyltin hydride (16.0 g, 55 mmol) and anhydrous ether (100 mL) according to the procedure of Example 6. Boiling point was 53°-55° C. at 0.7 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763552 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-7ba0a40bbe42467eb892804f5e745976 |
| Source note | uspto-grants-1998_06 |