HuagongsheHuagongshe Chemistry Print Report · For research reference only
Edetate Sodium → Ammonium Acrylate Acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Edetate Sodium | HCID 6144 | — |
| Reactant | tert-Butyl hydroperoxide | HCID 6410 | — |
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-(1,2-Dihydroxyethyl)oxolane-3,4-diol;octadec-9-enoic acid | HCID 57369882 | — |
| Solvent | Water | HCID 962 | — |
| Product | Ammonium Acrylate Acrylamide | HCID 86752756 | — |
Reaction Steps
An organic solution is prepared by combining a low odor paraffin oil (252.0 g), sorbitan sesquioleate (8.5 g) and polyoxyethylene sorbitol fatty acid (39.5 g) in a reactor with stirring. To this solution is added an aqueous solution of pH=8.0 containing acrylamide (84.0 g), acrylic acid (36.0 g) neutralized with aqueous ammonium hydroxide (35.7 g), tert-butyl hydroperoxide (0.048 g), ethylenediaminetetraacetic acid tetra sodium salt (0.24 g), and water (144.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763530 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-ad7bdabfcea94bdfa8c67d74fddc6758 |
| Source note | uspto-grants-1998_06 |