化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Edetate Sodium | HCID 6144 | — |
| 反応物 | Acrylamide | HCID 6579 | — |
| 反応物 | Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1) | HCID 162071 | — |
| 反応物 | Methyl 3-(1,3-benzodioxol-5-ylmethylsulfamoyl)thiophene-2-carboxylate | HCID 3476271 | — |
| 反応物 | Sodium Bromate | HCID 23668195 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride | HCID 155211 | — |
反応手順
An organic solution is prepared by combining a low odor paraffin oil (208.4 g), polyoxyethylene sorbitan monooleate (9.0 g) and polyoxyethylene sorbitan trioleate (32.6 g) in a reactor with stirring. To this solution is added an aqueous solution, adjusted to pH =3.5 with sulfuric acid, containing acrylamide (24.0 g), acryloxyethyltrimethyl ammonium chloride (80.2 g), sodium bromate (0.01 g), ethylenediaminetetraacetic acid tetra sodium salt (0.21 g), and water (145.58 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05763523 |
| 出典データセット | uspto-grants-1998_06 |
| ORD ID | ord-69d9a655d6d3497e8bf69b25d6566d6a |
| 出典メモ | uspto-grants-1998_06 |