HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 963601Generated: October 25, 2026
Glutaric Acid → Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride
https://huagongshe.com/reaction/963601
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Glutaric Acid | HCID 743 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Edetate Sodium | HCID 6144 | — |
| Reactant | tert-Butyl hydroperoxide | HCID 6410 | — |
| Reactant | Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1) | HCID 162071 | — |
| Reactant | Ammonium Sulfate | HCID 6097028 | — |
| Reactant | Span #80 (Sorbitan monooleate) | HCID 70693544 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride | HCID 155211 | — |
Reaction Steps
General polymerization procedure. AMD, acryloxyethyltrimethylammonium chloride, ammonium sulfate, glutaric acid solution, ethylenediaminetetraacetic acid tetra sodium salt solution, isopropanol, tert-butyl hydroperoxide solution, and Dl water are combined and the pH adjusted to 3.5 with sulfuric acid. Sorbitan monooleate is combined with low odor paraffin oil . The aqueous solution is slowly added to the oil solution and the combined mixture homogenized until a viscosity of 1200-1500 cps is obtained. The emulsion is sparged with nitrogen. The emulsion is heated to 40° C. The metabisulfite (MBS) solution is added at a rate to keep the reaction temperature between 40°-45° C. This is maintained until the reaction conversion is at least 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05763523 |
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| Source dataset | uspto-grants-1998_06 |
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| ORD ID | ord-25e19dc6bc614718a18d147526cd67a0 |
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| Source note | uspto-grants-1998_06 |
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