Dichloromethane → HCID 86752775, compound

HRID 963793Notes

Reaction equation

HRID 963793 reaction equation
[F:1][C:2]1[C:9]([F:10])=[C:8]([O:11][CH2:12][O:13][CH2:14][CH2:15][O:16][CH3:17])[C:7]([O:18][CH2:19][O:20][CH2:21][CH2:22][O:23][CH3:24])=[CH:6][C:3]=1[CH:4]=[CH2:5].C(Cl)Cl.ClCCl.C(OCC)(=[O:33])C>>[F:1][C:2]12[O:33][C:3]1([CH:6]=[C:7]([O:18][CH2:19][O:20][CH2:21][CH2:22][O:23][CH3:24])[C:8]([O:11][CH2:12][O:13][CH2:14][CH2:15][O:16][CH3:17])=[C:9]2[F:10])[CH:4]=[CH2:5]

Participants

4

Reactant 3

HCID 6344DichloromethaneHCID 18359058HCID 18359058, compoundHCID 21226138Dichloromethane ethylacetate

Product 1

HCID 86752775HCID 86752775, compound

Procedure

Using the procedure of Stage D of Example 40, 32 g of the product of Stage E were reacted to obtain 33.5 g of the expected product with a Rf=0.14 (CH2Cl2 --AcOEt 8-2).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-eeff55f789df4c27a5a5f748e8347b31
Source dataset
uspto-grants-1998_06
Patent number
US05763617

Reaction notes

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