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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 963794Generated: October 26, 2026

Diisobutylaluminumhydride → 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol

https://huagongshe.com/reaction/963794

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisobutylaluminumhydrideHCID 21225700—
Reactant2,3,Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styryl carboxylateHCID 131719753—
Product2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrolHCID 1835916599.6%

Reaction Steps

Using the procedure of Stage C of Example 40, 20 g of ester of Step B and 88 ml of diisobutylaluminium hydride were reacted to obtain 17.9 g of the expected product melting at 60° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05763617
Source datasetuspto-grants-1998_06
ORD IDord-6a19ae352ae24746a267fabdf73cbf09
Source noteuspto-grants-1998_06