HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichlorohexafluorocyclobutane → 1-Chloro 3,3,4,4-tetrafluoro cyclobutene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichlorohexafluorocyclobutane | HCID 9643 | — |
| Reactant | Hexafluorocyclobutene | HCID 12767 | — |
| Product | 1-Chloro 3,3,4,4-tetrafluoro cyclobutene | HCID 12663854 | — |
Reaction Steps
The conversion of 1,2-dichlorohexafluorocyclobutane was 30%, the selectivity of the targeted hexafluorocyclobutene was 96% and a 3.5% selectivity of tetrafluoro-1-chlorocyclobutene was formed as the by-product. The selectivity and the conversion were calculated by multiplying the correction coefficient, which was independently determined by the gas chromatography peak areas. The same procedure was used for the following operations.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763703 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-aba3804530b64007a937b59926300bb1 |
| Source note | uspto-grants-1998_06 |