HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 226704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2-Ethylphenol | HCID 6997 | — |
| Reactant | Hexane, 2,5-dichloro-2,5-dimethyl- | HCID 80360 | — |
| Product | HCID 226704 | HCID 226704 | — |
Reaction Steps
In a manner similar to Example 7 (a) above, by the reaction of 15 g (0.123 mol) of 2-ethylphenol with 22.5 g (0.123 mol) of 2,5-dichloro-2,5-dimethylhexane, 25.4 g (89%) of the expected phenol of melting point 88°-9° C. were obtained after chromatography on a silica column eluted with dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05766610 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-32fa81636f734108a93d73253ee765b9 |
| Source note | uspto-grants-1998_06 |