HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2,2-Dimethyl-4-benzyloxycarbonylbutyryl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,2-Dimethyl-4-benzyloxycarbonylbutyric acid | HCID 19080045 | — |
| Product | 2,2-Dimethyl-4-benzyloxycarbonylbutyryl chloride | HCID 19080038 | — |
Reaction Steps
A mixture of 3.1 g of 2,2-dimethyl-4-benzyloxycarbonylbutyric acid and 3.3 ml of oxalyl chloride was refuxed for 1 h. After being cooled to room temperature, the solution was concentrated in vacuo and dried overnight The obtained oil was not further purified for the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05767256 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-3e46a729568240518792c9616546daaf |
| Source note | uspto-grants-1998_06 |