Chlorotrimethylsilane → HCID 54286423, compound

Participants

Reaction Steps

A solution of phenyl (hydroxy)thioacetate (0.237 g, 1.41 mmol) in THF (14.0 ml) was treated with trimethylsilyl chloride (0.643 ml, 5.07 mmol) and triethylamine (0.726 ml, 5.21 mmol) at room temperature. After stirring for 2 h at RT, the mixture was diluted with ethyl ether, washed with pH 7 phosphate buffer, dried (Na2SO4) and evaporated to give phenyl (trimethylsilyloxy)thioacetate (0.2315 g, 93%).

Provenance & Evidence