Sodium Methoxide → HCID 86752792, compound

Participants

Reaction Steps

A solution of 1.0 g of (naphthalene-2,6-dicarboxylic acid bis- [(benzyl 3,4,6-tri-O-acetyl-2-desoxy-α-D-glucopyranosid-2-yl)-amide] in 20 ml of methanol and 20 ml of dioxan was stirred at room temperature for 18 hours with ml of a 0.3M sodium methanolate solution. The resulting precipitate was washed with methanol, dioxan and ether, dried and gave naphthalene-2,6-dicarboxylic acid bis-[(benzyl 2-desoxy-α-D-glucopyranosid-2-yl)-amide], MS: m/z 717.2 ([M-H]-).

Provenance & Evidence