HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86752813, compound → HCID 86752812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86752813 | HCID 86752813 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86752812 | HCID 86752812 | — |
Reaction Steps
2,3,4,5,6-Penta-O-acetyl-L-gulonic acid (benzyl 3,4-di-O-acetyl-2-benzyloxycarbonylamino-2,6-didesoxy-α-D-glucopyranosid-6-yl)-amide was hydrogenated as described under Ex. 13.B. and gave 2,3,4,5,6-penta-O-acetyl-L-gulonic acid (benzyl 3,4-di-O-acetyl-2-amino-2,6-didesoxy-α-D-glucopyranosid-6-yl)-amide, [α]+75.50 (c 0.2; dioxan), MS: m/z 763.6 ([M+Na]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05767268 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-7e81bbef35de4f02ab783033a284034d |
| Source note | uspto-grants-1998_06 |