HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ozone → HCID 54235645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ozone | HCID 24823 | — |
| Reactant | 3-{4-[(Prop-2-en-1-yl)oxy]phenyl}propanoic acid | HCID 19348982 | — |
| Product | HCID 54235645 | HCID 54235645 | 82% |
Reaction Steps
4-(2-Propenyloxy)benzenepropanoic acid (120 mg, 0.58 mmol) is treated with ozone by the procedure described in Example 2 to give 100 mg (82%) of 4-(2-oxoethoxy)benzenepropanoic acid as a white powder: m.p. 95°-100°; the 1H NMR (300 MHz, CDCl3) is consistent with the desired product; IR (KBr) 3400, 1740, 1720, 1610 cm-1 ; MS (CI low res) m/e 207, 191, 179, 165, 149.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05767285 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-14a05c67ec1040739b247ad88698a277 |
| Source note | uspto-grants-1998_06 |