HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentafluorobenzoyl chloride → HCID 19074002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentafluorobenzoyl chloride | HCID 75256 | — |
| Reactant | HCID 19074016 | HCID 19074016 | — |
| Product | HCID 19074002 | HCID 19074002 | — |
Reaction Steps
4-Aminomethyl-7-diethylaminocoumarin (50 mg, 0.2 mmol) is treated with pentafluorobenzoyl chloride (0.5 mL, 0.3 mmol) at 0° C. under dry argon protection, and worked up according to the procedure of Example 25. Compound 29 is obtained as an off-white solid (67 mg, yield: 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05773236 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-2375d12931f44f92b3945b9fac9b828b |
| Source note | uspto-grants-1998_06 |