Methyl iodide → 131988-13-1

HRID 965026Notes

Reaction equation

HRID 965026 reaction equation
[CH3:1][I:2].[CH2:3]([O:6][C:7]1[C:11]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:10][S:9][N:8]=1)[CH2:4][CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:6][C:7]1[C:11]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:10][S:9][N:8]=1)[CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180132HCID 15180132, compound

Product 1

HCID 15819045131988-13-1

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.37 ml, 6 mmol) and 3-(3-propoxy-1,2,5-thiadiazol-4-yl)pyridine (700 mg, 3.1 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.98 g (88%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.98 g (88%)

Sources & evidence

ORD record
ord-2831a8113fa3466f9286507f4697e4f4
Source dataset
uspto-grants-1998_06
Patent number
US05773452

Reaction notes

Loading…