HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(4-Chloro-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-Chloro-4-(pyridin-3-yl)-1,2,5-thiadiazole | HCID 10488164 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(4-Chloro-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide | HCID 19075334 | 100.1% |
Reaction Steps
A solution of 3-(3-chloro-1,2,5-thiadiazol-4-yl)pyridine (1.98 g, 10 mmol) and methyl iodide (4.25 g, 30 mmol) in acetone (10 ml) was stirred at room temperature for 16 h. The precipitate was collected by filtration to yield 3.40 g (100%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05773452 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-2c6edade2cc04703a6d53d3e65cb58c4 |
| Source note | uspto-grants-1998_06 |