Methyl iodide → HCID 19075355, compound

HRID 965086Notes

Reaction equation

HRID 965086 reaction equation
[CH3:1][I:2].[O:3]1[CH2:8][CH2:7][N:6]([C:9]2[C:13]([C:14]3[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=3)=[N:12][S:11][N:10]=2)[CH2:5][CH2:4]1>CC(C)=O>[I-:2].[O:3]1[CH2:4][CH2:5][N:6]([C:9]2[C:13]([C:14]3[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=3)=[N:12][S:11][N:10]=2)[CH2:7][CH2:8]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075225HCID 19075225, compound

Product 1

HCID 19075355HCID 19075355, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(3-morpholino-1,2,5-thiadiazol-4-yl)pyridine (680 mg, 2.7 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 1.0 g (94%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 1.0 g (94%)

Sources & evidence

ORD record
ord-d9b0826db4a249bea066b02d02091f48
Source dataset
uspto-grants-1998_06
Patent number
US05773452

Reaction notes

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