Methyl iodide → HCID 19075218, compound
Reaction equation
[CH3:1][I:2].[CH2:3]([S:7][C:8]1[C:12]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH2:4][CH2:5][CH3:6]>>[I-:2].[CH2:3]([S:7][C:8]1[C:12]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH2:4][CH2:5][CH3:6]Participants
3
Procedure
Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-butylthio-1,2,5-thiadiazol-4-yl)pyridine (0.6 g, 2.3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-ef6bd72af29f4fb7a561241c30ae777b
- Source dataset
- uspto-grants-1998_06
- Patent number
- US05773452
Reaction notes
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