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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 965123Generated: November 1, 2026

Methyl iodide → 3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-1,6-dimethylpyridinium iodide

https://huagongshe.com/reaction/965123

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
Reactant3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-6-methylpyridineHCID 19075369—
SolventAcetoneHCID 180—
Product3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-1,6-dimethylpyridinium iodideHCID 19075328—

Reaction Steps

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-hexylthio-1,2,5-thiadiazol-4-yl)-6-methylpyridine (4 mmol) in acetone (5 ml) and the reaction mixture was stirred at room temperature for 20 h. Evaporation of the reaction mixture gave the crude product, which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05773452
Source datasetuspto-grants-1998_06
ORD IDord-7cc851cb76cf4fac8cf4701e2deeacb4
Source noteuspto-grants-1998_06