Dibutyl Phthalate → 2-Hydroxyethyl Methacrylate

HRID 965267Notes

Reaction equation

HRID 965267 reaction equation
CCCCCCCC(OOC(C)(C)C)=[O:9].C(OCCCC)(=O)[C:17]1[C:18](=[CH:26]C=CC=1)[C:19]([O:21][CH2:22][CH2:23]CC)=[O:20]>>[C:19]([O:21][CH2:22][CH2:23][OH:9])(=[O:20])[C:18]([CH3:17])=[CH2:26]

Participants

3

Reactant 2

HCID 3026Dibutyl PhthalateHCID 83499Octaneperoxoic acid, 1,1-dimethylethyl ester

Product 1

HCID 133602-Hydroxyethyl Methacrylate

Procedure

2 h after the end of the addition, 1 g of tert-butyl peroctoate is fed in. The total polymerization time is 8 h. After the end of polymerization, the mixture is diluted with 590.0 g of dibutyl phthalate. An almost clear, viscous solution is obtained.

Workup

  1. customAfter the end of polymerization
  2. customAn almost clear, viscous solution is obtained

Sources & evidence

ORD record
ord-4e8d258d76fe4ab7af350548402b97c8
Source dataset
uspto-grants-1998_06
Patent number
US05773505

Reaction notes

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