2-(2-Chloroethoxy)tetrahydro-2H-pyran → HCID 22116122, compound
Reaction equation
[CH2:1]([C:3]1([CH3:13])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[NH:5][C:4]1=[O:12])[CH3:2].Cl[CH2:15][CH2:16][O:17]C1CCCCO1>>[CH2:1]([C:3]1([CH3:13])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]([CH2:15][CH2:16][OH:17])[C:4]1=[O:12])[CH3:2]Participants
3
Procedure
Prepared from 3-ethyl-3-methyl-1,3-dihydro-2H-indol-2-one (prepared by the method of Endler and Becker; Organic Syntheses Coll. vol. 4 page 657) and 2-(2-chloroethoxy) tetrahydro-2H-pyran.
Workup
- customprepared by the method of Endler and Becker
Sources & evidence
- ORD record
- ord-b9479e76cd724464b461417ed6565f98
- Source dataset
- uspto-grants-1998_06
- Patent number
- US05773448
Reaction notes
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