Carbon Dioxide → HCID 54358079, compound

HRID 965320Notes

Reaction equation

HRID 965320 reaction equation
[CH2:1]([O:3][C:4](=[O:37])[C:5](=[NH:36])[CH:6](P(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH3:2].[C:38](=O)=[O:39]>>[CH2:1]([O:3][C:4](=[O:37])[CH:5]([N:36]=[C:38]=[O:39])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:14])([CH3:15])[CH3:16])=[O:11])[CH3:2]

Participants

3

Reactant 2

HCID 280Carbon DioxideHCID 178472716HCID 178472716, compound

Product 1

HCID 54358079HCID 54358079, compound

Conditions

Temperature
50 °C

Procedure

The reaction solution from Example 9 is placed in a Parr® bomb and carbon dioxide (22 g, 0.5 mol) is condensed into the bomb. The bomb is sealed and heated to 50° C. for 12 hours. The bomb is cooled and vented to atmospheric pressure. The solution is transferred from the bomb to a flask and used as is in the next reaction (Example 11).

Workup

  1. customcondensed into the bomb
  2. customThe bomb is sealed
  3. temperatureThe bomb is cooled
  4. customThe solution is transferred from the bomb to a flask
  5. customas is in the next reaction (Example 11)

Sources & evidence

ORD record
ord-4aea66748c58497d8c3f804e2902be7e
Source dataset
uspto-grants-1998_06
Patent number
US05773571

Reaction notes

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