反应详情

温度

50 °C

The reaction solution from Example 9 is placed in a Parr® bomb and carbon dioxide (22 g, 0.5 mol) is condensed into the bomb. The bomb is sealed and heated to 50° C. for 12 hours. The bomb is cooled and vented to atmospheric pressure. The solution is transferred from the bomb to a flask and used as is in the next reaction (Example 11).

1. customcondensed into the bomb
2. customThe bomb is sealed
3. temperatureThe bomb is cooled
4. customThe solution is transferred from the bomb to a flask
5. customas is in the next reaction (Example 11)