Hydrochloric Acid → HCID 131723436, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of the compound of Example 198, Step D (12 mg) in EtOH (2 mL, 0° C.) was added conc. HCl (0.2 mL). The solution was stirred at 0° C. for 1 h and concentrated down to deliver 10 mg of Example 198, Step E: +APcI MS (M+1)+ 544; 1H NMR=400 MHz (CD3OD) δ: 7.31 (br m, 6H), 6.83 (m, 2H), 2.59 (br s, 3H), 1.56 (br s, 6H).

Provenance & Evidence