HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22957171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57147632 | HCID 57147632 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22957171 | HCID 22957171 | — |
Reaction Steps
Compound of Example 202, Step E (12 mg, 0.020 mmol) was deprotected as described in General Procedure C to provide, after trituration with ether, Example 202, Step F as its HCl salt (5 mg, 50%): +APcI MS (M+1)+ 494; 1H NMR (400 MHz, CD3OD) δ: 8.90-7.15 (arom, series of m, 9 H), 5.31 (m, 0.5H), 5.15 (m, 0.5H), 2.86 (d, 0.5H), 2.77 (d, 0.5H), 1,60 (Me, m, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951850B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-0e5f0d095ccd49c38157e03978e6264a |
| Source note | uspto-grants-2005_10 |