HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide → N-(3-Butynyl)phthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | 3-Butyn-1-OL | HCID 13566 | — |
| Reactant | HCID 15530194 | HCID 15530194 | — |
| Product | N-(3-Butynyl)phthalimide | HCID 11171619 | 84% |
Reaction Steps
The title compound was prepared according to the procedure of lyer and Liebeskind (J. Amer. Chem. Soc, 1987, 109, 2759-2770) via a Mitsunobu reaction between phthalimide and 3-butyn-1-ol in 84% yield. The product was isolated as white crystals. mp=137-139° C. (lit. mp=136-137° C.). N-(Ethoxycarbonyl)but-3-ynylamine
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951863B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-47c3f604df774a589fbb08063b20dd3f |
| Source note | uspto-grants-2005_10 |