HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentylamine → HCID 22313254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | 4-chloro-5-ethyl-6-methylpyrimidin-2-amine | HCID 676462 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22313254 | HCID 22313254 | 58.1% |
Reaction Steps
A mixture of 4-chloro-5-ethyl-6-methylpyrimidine-2-ylamine (400 mg, 33 mmol), amylamine (1.35 ml) and dioxane (5 ml) was kept at 95-100° C. for 17 hours. The procedure according to pro-treatment of Example 23 was carried out to give the object compound (301 mg, 58.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951866B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-a4d4814f05fa4c31888e55cc2e3f55ca |
| Source note | uspto-grants-2005_10 |