HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentylamine → HCID 22313255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | HCID 22313251 | HCID 22313251 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22313255 | HCID 22313255 | 79.7% |
Reaction Steps
A mixture of 4-chloro-5-phenethylpyrimidine-2-ylamine (234 mg, 1 mmol), amylamine (0.58 ml) and dioxane (2 ml) was kept at 95-100° C. for 8.5 hours. The procedure according to pro-treatment of Example 27 was carried out to give the object compound (227 mg, 79.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951866B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-e237e36d89834703a8ae8dfb2ace915e |
| Source note | uspto-grants-2005_10 |