HRID965745

反应详情

EQUATION

反应方程式

HRID 965745 的结构方程式

PROCEDURE

实验过程

Following General Procedure A above using N-(3,5-difluorophenylacetyl)-L-alanine (Example B) and 1-amino-3-methyl-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one, the title compound was prepared. The reaction was monitored by tlc on silica gel (Rf=0.15 in ethyl acetate) and purification was by flash chromatography using ethyl acetate as the eluant.

WORKUP

后处理

  1. customThe reaction was monitored by tlc on silica gel (Rf=0.15 in ethyl acetate) and purification