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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 965865Generated: October 29, 2026

Dimethyl Sulfate → HCID 69592128, compound

https://huagongshe.com/reaction/965865

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfateHCID 6497—
ReactantSodium CyanideHCID 8929—
ReactantHCID 69592105HCID 69592105—
ProductHCID 69592128HCID 69592128—

Reaction Steps

Following the general method described in example 2b, 2-[2-(2-fluoro-phenyl)-vinyl]-pyridine 1-oxide was reacted first with dimethylsulfate and then with NaCN. After extraction and crystallisation the title compound was obtained as a brown crystalline material. MS: m/e=224 (M+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06951875B2
Source datasetuspto-grants-2005_10
ORD IDord-803256fede224ae9a77997660dbd9cde
Source noteuspto-grants-2005_10