HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 22176442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 69592084 | HCID 69592084 | — |
| Product | HCID 22176442 | HCID 22176442 | — |
Reaction Steps
Following, the general method described in example 2b, 2-methyl-4-styryl-pyridine 1-oxide was reacted first with dimethylsulfate and then with NaCN. After extraction and chromatography (SiO2 with CH2Cl2) the title compound was obtained as a yellow crystalline material. MS: m/e=220 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951875B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-6af1829152ed4b3bbf64181a483ca659 |
| Source note | uspto-grants-2005_10 |