HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22249494, compound → HCID 22249612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22249494 | HCID 22249494 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22249612 | HCID 22249612 | 84.6% |
Reaction Steps
Activated manganese dioxide (45 mg, 0.51 mmol) was added to a solution of 1-(1-ethylpropyl)-7-iodo-4-mesityl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline (39 mg, 0.10 mmol) in toluene (4.0 mL) and methylene chloride (4.0 mL), followed by heating under reflux for one day. The mixture was filtered through Celite and evaporated, to give the title compound (32 mg) as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951865B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-8eeca6a6e68a4f1d98f0a88db91f7f81 |
| Source note | uspto-grants-2005_10 |