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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 966026Generated: October 31, 2026

HCID 22249494, compound → HCID 22249612, compound

https://huagongshe.com/reaction/966026

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22249494HCID 22249494—
CatalystHCID 178418406HCID 178418406—
SolventTolueneHCID 1140—
SolventDichloromethaneHCID 6344—
ProductHCID 22249612HCID 2224961284.6%

Reaction Steps

Activated manganese dioxide (45 mg, 0.51 mmol) was added to a solution of 1-(1-ethylpropyl)-7-iodo-4-mesityl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline (39 mg, 0.10 mmol) in toluene (4.0 mL) and methylene chloride (4.0 mL), followed by heating under reflux for one day. The mixture was filtered through Celite and evaporated, to give the title compound (32 mg) as pale yellow crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06951865B2
Source datasetuspto-grants-2005_10
ORD IDord-8eeca6a6e68a4f1d98f0a88db91f7f81
Source noteuspto-grants-2005_10