HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 6,8-Bis(acetylthio)octanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 6,8-Bisacetylmercaptooctanoic acetic anhydride | HCID 86585610 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 6,8-Bis(acetylthio)octanoic acid | HCID 9926084 | — |
Reaction Steps
The anhydride from step 2 (8.0 g) was mixed with 30 mL of water and 30 mL of 2-propanol and stirred at 40 for 4.25 hr. After about 2 hr there was a clear solution. The solvent was evaporated under vacuum (2 mm) at 25. The oil remaining was evaporated with 10 mL of water to remove any residual 2-propanol and acetic acid. An almost colorless oil weighing 6.8 g was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951887B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-1144bbf5839348aba727310ab433b030 |
| Source note | uspto-grants-2005_10 |