2,6-Di-tert-butyl-4-methylphenol → HCID 178506937, compound

Participants

Reaction Steps

Both 10 mmol (2.2 g) of monocyclopentadienyl titanium chloride(CpTiCl3) and 100 ml of toluene were added to a 200 ml Schlenk reactor in the inert atmosphere. Then, 10 mmol of 2,6-di-t-butyl 4-methyl phenoxy lithium, so obtained from the reaction between 2,6-di-t-butyl 4-methyl phenol and n-butyl lithium, was slowly added to the mixture. The reactional solution was stirred at room temperature and stood for 1 hour. After 1 hour, some portions of the mixture we collected ad were analyzed by 1H-NMR spectroscopy to ascertain the reaction results.

Provenance & Evidence