Diethylamine → HCID 23393788, compound

Participants

Reaction Steps

To a solution of the product of Step A (58 mg, 0.14 mmol) in dioxane (1 mL) was added diethyl amine (0.14 mL, 1.4 mmol) and the resultant solution was heated at 70° C. overnight. The reaction solution was concentrated in vacuo and the crude product purified by flash chromatography (9:1 Ethyl Acetate:Methanol w/0.5% triethylamine) to provide the compound (44 mg, 80%) as a yellow oil. LC/MS (ESL+) 397 (M+1).

Provenance & Evidence