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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 967006Generated: October 30, 2026

Hydrochloric Acid → HCID 22957171, compound

https://huagongshe.com/reaction/967006

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57147632HCID 57147632—
SolventDiethyl EtherHCID 3283—
ProductHCID 22957171HCID 22957171—

Reaction Steps

Compound of Example 202, Step E (12 mg, 0.020 mmol) was deprotected as described in General Procedure C to provide, after trituration with ether, Example 202, Step F as its HCl salt (5 mg, 50%): +APcI MS (M+1)+ 494; 1H NMR (400 MHz, CD3OD) δ: 8.90-7.15 (arom, series of m, 9H), 5.31 (m, 0.5H), 5.15 (m, 0.5H), 2.86 (d, 0.5H), 2.77 (d, 0.5H), 1.60 (Me, m, 6H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06953791B2
Source datasetuspto-grants-2005_10
ORD IDord-7219fb3c808041e2ba83454085220b37
Source noteuspto-grants-2005_10