HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → HCID 22254467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | HCID 22254498 | HCID 22254498 | — |
| Product | HCID 22254467 | HCID 22254467 | 94.2% |
Reaction Steps
Using the general method of Example 1 Part 2-[2-(methoxyethyl)-1H-imidazo[4,5-c]quinolin-1-yl]ethanol (2.53 g, 9.33 mmol) was reacted with propargyl bromide (80% in toluene, 3.11 mL, 27.9 mmol) to provide 2.72 g of 2-(methoxyethyl)-1-[2-(prop-2-ynyloxy)ethyl]-1H-imidazo[4,5-c]quinoline as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953804B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-847c6304243043e0801ce1f469879a57 |
| Source note | uspto-grants-2005_10 |