4-Chlorophenyl chloroformate → HCID 178484033, compound

Participants

Reaction Steps

In analogy to the procedure described in example 1.7, 0.325 g (1.90 mmol) of trans-2-(4-methylaminomethyl-cyclohexyl)-ethanol were acylated with 0.54 g (2.84 mmol) of 4-chlorophenyl chloroformate to yield 0.34 g (55%) trans-[4-(2-hydroxy-ethyl)-cyclohexylmethyl]-methyl-carbamic acid 4-chloro-phenyl ester as colorless viscous oil, MS: 326 (MH+, 1Cl).

Provenance & Evidence