HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 178483626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 178483623 | HCID 178483623 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178483626 | HCID 178483626 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester was reacted with piperidine in N,N-dimethylacetamide at room temperature to yield trans-methyl-{2-[4-(3-piperidin-1-yl-(E)-propenyl)-cyclohexyl]-ethyl}-carbamic acid 4-chloro-phenyl ester as colorless viscous oil, MS: 419 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-c57cd253c5514377a3eb8ae7633b7875 |
| Source note | uspto-grants-2005_10 |