HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 178483454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 178483624 | HCID 178483624 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178483454 | HCID 178483454 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-N-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide was reacted with dimethyl-amine in N,N-dimethylacetamide at room temperature to yield trans-N-{2-[4-(3-dimethylamino-(E)-propenyl)-cyclohexyl]-ethyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide as colorless viscous oil, MS: 433 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-8e6339bcd380490698d4e6366394c78a |
| Source note | uspto-grants-2005_10 |