HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 178483453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 178483623 | HCID 178483623 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178483453 | HCID 178483453 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester was reacted with dimethylamine in N,N-dimethylacetamide at room temperature to yield trans-{2-[4-(3-dimethylamino-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester as light yellow viscous oil, MS: 379 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-710bb1e46f22415f88fa90283d5feaaa |
| Source note | uspto-grants-2005_10 |