HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 178464017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 178483623 | HCID 178483623 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178464017 | HCID 178464017 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester was reacted with ethylamine in N,N-dimethylacetamide at room temperature to yield trans-{2-[4-(3-ethylamino-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester as light yellow viscous oil, MS: 379 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-4b47a3b7852d400eb6a384a1e01d0fef |
| Source note | uspto-grants-2005_10 |