HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 178484066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | HCID 178484053 | HCID 178484053 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178484066 | HCID 178484066 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-N-[4-(4-bromo-(E)-but-2-enyloxymethyl)-cyclohexylmethyl]-N-methyl-4-trifluoromethyl-benzenesulfonamide was reacted with bis-(2-hydroxy-ethyl)-amine in N,N-dimethylacetamide at room temperature to yield trans-N-(4-{4-[bis-(2-hydroxy-ethyl)-amino]-(E)-but-2-enyloxymethyl}-cyclohexylmethyl)-N-methyl-4-trifluoromethyl-benzenesulfonamide as light yellow solid, MS: 523 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-33c1e3b4736f4445958d6bef1fd390d1 |
| Source note | uspto-grants-2005_10 |